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Дата издания
16.06.2025Область исследования
Тип исследования
Аннотация (краткое описание)
This study explores the potential of oil sludge, a hazardous by-product of the oil industry, as a sustainable rejuvenator for restoring the physicochemical and rheological properties of aged bitumen. Aged binder samples were modified with different concentrations of oil sludge (1%, 3%, and 5%) and analyzed using dynamic shear rheometry (DSR), Fourier-transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), and thermogravimetric analysis (TGA). The incorporation of 5% oil sludge increased penetration from 60 to 71 mm and the softening point from 55 °C to 72 °C, indicating enhanced flexibility. DSR measurements showed a ~10% decrease in complex modulus (G*) and a slight increase in phase angle, confirming partial rheological recovery. FTIR spectra revealed partial restoration of aliphatic and aromatic functional groups, with a decrease in sulfoxide absorption bands, while SEM analysis indicated improved homogeneity and reduced microcracking. TGA confirmed enhanced thermal behavior and a reduction in residual mass. The novelty of this work lies in the first-time application of regionally sourced oil sludge as a rejuvenator, evaluated through a multiscale analytical framework. These findings demonstrate the dual benefits of performance recovery and hazardous waste valorization, contributing to sustainable road maintenance within a circular economy approach. © 2025 by the authors.DOI
10.3390/app15126757Тип публикаций
Сведения о финансировании
Ministry of Education and Science of the Republic of Kazakhstan, №AP22786142, BR27199103Данный документ располагается в коллекциях
Международные публикации ученых SU
Scopus
Файлы документа
applsci-15-06757.pdf